• 专利标题:   Preparing self-supporting porous nitrogen-doped graphene network lithium metal main body material comprises e.g. adding vat red F3B dye to graphene oxide suspension, ultrasonically and uniformly stirring, pouring mixed solution into template, and placing it into oven to self-assemble into film.
  • 专利号:   CN115241445-A
  • 发明人:   DU Z, HE C, AI W
  • 专利权人:   UNIV NORTHWESTERN POLYTECHNICAL NINGBO
  • 国际专利分类:   H01M004/36, H01M004/38, H01M004/583, H01M004/62
  • 专利详细信息:   CN115241445-A 25 Oct 2022 H01M-004/36 202301 Chinese
  • 申请详细信息:   CN115241445-A CN11040199 29 Aug 2022
  • 优先权号:   CN11040199

▎ 摘  要

NOVELTY - Preparing self-supporting porous nitrogen-doped graphene network lithium metal main body material comprises (1) dispersing graphene oxide in deionized water, ultrasonically dispersing to form a suspension, and obtaining a graphene oxide suspension, (2) adding vat red F3B dye to the graphene oxide suspension obtained in step (1), ultrasonically and uniformly stirring to obtain a mixed solution, (3) pouring the mixed solution obtained in step (2) into the template, placing it into an oven to self-assemble into a film through the liquid-gas interface, where the temperature is 35-90°C, and obtaining self-supporting composite film, and (4) heat-treating the composite film in step (3) under a protective atmosphere, where the heat treatment temperature is 300-1000°C for 0.5-5 hours and the heating rate is 1-15°C/minutes, and obtaining self-supporting porous nitrogen-doped graphene network lithium metal main body material. USE - The method is useful for preparing self-supporting porous nitrogen-doped graphene network lithium metal main body material. ADVANTAGE - The method realizes the high-rate performance of the lithium metal battery, promotes the development of the lithium metal battery, provides novel self-supporting lithium metal main body material for fast charging and discharging, and is easy to operate and can be prepared on a large scale. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for self-supporting porous nitrogen-doped graphene network lithium metal main body material prepared by the above preparation method.