• 专利标题:   Graphene oxide-polyglycerol fatty acid ester composite modified nano-calcium carbonate powder useful as reinforcing filler, contains calcium oxide, carbon dioxide, polyglycerol fatty acid ester, ionic liquid and graphene oxide.
  • 专利号:   CN106752101-A
  • 发明人:   WANG W
  • 专利权人:   QINGYANG JINSHAN POWDER IND CO LTD
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01F011/18, C09C001/02, C09C003/06, C09C003/10
  • 专利详细信息:   CN106752101-A 31 May 2017 C09C-001/02 201750 Pages: 4 Chinese
  • 申请详细信息:   CN106752101-A CN10919718 21 Oct 2016
  • 优先权号:   CN10919718

▎ 摘  要

NOVELTY - A graphene oxide-polyglycerol fatty acid ester composite modified nano-calcium carbonate powder contains 30-50 pts. wt. calcium oxide, balance amount of carbon dioxide, 0.2-0.5 pt. wt. polyglycerol fatty acid ester, 200-500 pts. wt. deionized water, 1-20 pts. wt. ionic liquid and 0.01-0.02 pt. wt. graphene oxide. USE - The graphene oxide-polyglycerol fatty acid ester composite modified nano-calcium carbonate powder is useful as reinforcing filler. ADVANTAGE - The graphene oxide-polyglycerol fatty acid ester composite modified nano-calcium carbonate powder has excellent dispersibility, controllability and toughening and reinforcing effect. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation method of graphene oxide-polyglycerol fatty acid ester composite modified nano-calcium carbonate powder, which involves uniformly dispersing graphene oxide and polyglycerol fatty acid ester in deionized water, heating at 70-80 degrees C and stirring to prepare emulsified liquid, adding ionic liquid and deionized water to reaction container and stirring under nitrogen atmosphere for 40-50 minutes, heating at 80-85 degrees C, then adding calcium oxide, grinding and stirring for 2-3 hours to form calcium hydroxide slurry and aging for 10-15 hours, injecting the composite emulsion in calcium hydroxide slurry, stirring and uniformly mixing, introducing carbon dioxide gas, stirring, continuously stirring and mixing for 60-80 minutes after finishing reaction, filtering, washing filtrate, vacuum drying and dispersing.