• 专利标题:   Preparing heat dissipation film based on large-diameter graphene oxide comprises e.g. stirring modified graphene oxide, modified boron nitride, modified carbon nanotube and solvent into reactor, reacting and casting polycondensate into film.
  • 专利号:   CN112920604-A, CN112920604-B
  • 发明人:   CUI J, XU P, LI Y, ZHANG B
  • 专利权人:   XU P, JIANGSU XINGTU NEW MATERIAL TECHNOLOGY
  • 国际专利分类:   C01B021/064, C01B032/168, C01B032/198, C08G073/10, C08J005/18, C08K003/04, C08K003/38, C08K009/02, C08K009/04, C08K009/06, C08L077/10, C08L079/08
  • 专利详细信息:   CN112920604-A 08 Jun 2021 C08L-079/08 202160 Pages: 11 Chinese
  • 申请详细信息:   CN112920604-A CN10168171 07 Feb 2021
  • 优先权号:   CN10168171

▎ 摘  要

NOVELTY - Preparing heat dissipation film based on large-diameter graphene oxide comprises (i) adopting 40-50 pts. wt. diamine monomer, 40-50 pts. wt. dianhydride monomer, 3 pts. wt. modified graphene oxide, 3 pts. wt. modified boron nitride, 5 pts. wt. aramid fiber, 3 pts. wt. modified carbon nano-tubes and 40-50 pts. wt. solvent, (ii) stirring modified graphene oxide, modified boron nitride, modified carbon nanotubes and solvent into the reactor under the condition of rotation speed 200-300 revolutions/minute for 30 minutes, adding diamine monomer and dianhydride monomer to the reaction kettle, heating to 30-40 degrees C with rotation speed unchanged, stirring and reacting for 1-2 hours to obtain polycondensate, and (iii) casting polycondensate into a film, drying at 80 degrees C for 2 hours, heating up to 300-400 degrees C at a heating rate of 3 degrees C/minute, drying for 10 minutes to obtain a polyamic acid film, and transversely and longitudinally stretching to obtain a heat dissipation film. USE - The method is useful for preparing a heat dissipation film based on large-diameter graphene oxide. ADVANTAGE - The heat dissipation film has good mechanical and flame retardant properties.