• 专利标题:   Preparing graphene by ammonia heat batch method comprises e.g. adding graphite powder into reactor filled with ammonia gas, adding aqueous ammonia, heating, vacuum extracting, cooling, absorbing material, filtering solution and drying.
  • 专利号:   CN108314012-A
  • 发明人:   SUN L, MA Y, LI D
  • 专利权人:   SHANDONG HENGHUA NEW MATERIALS CO LTD
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN108314012-A 24 Jul 2018 C01B-032/184 201853 Pages: 7 Chinese
  • 申请详细信息:   CN108314012-A CN10029989 16 Jan 2017
  • 优先权号:   CN10029989

▎ 摘  要

NOVELTY - Preparing graphene by ammonia heat batch method comprises (i) adding graphite powder into reactor filled with ammonia gas, (ii) adding aqueous ammonia into reaction vessel of step (i) and stirring to obtain mixed liquid, (iii) heating and maintaining the reactor of step (ii), (iv) vacuum extracting and cooling using water, and absorbing the material in reactor of step (iii) to obtain aqueous ammonia solution containing graphene, and (v) filtering solution obtained in step (iv) and drying to obtain graphene product. USE - The method is useful for preparing graphene by ammonia heat batch method. ADVANTAGE - The graphene has excellent electrochemical performance; and is suitable for industrial production.