• 专利标题:   Preparing graphene in-situ polymerization modified polyamide epoxy curing agent involves adding dibasic acid and graphene to reactor, raising temperature while stirring, thermostating and sonicating, and adding polyamine to reaction vessel.
  • 专利号:   CN110204707-A
  • 发明人:   WAN Y, ZHENG J, ZHOU L, JIANG W, CAO J, LIU X, MA H, ZHAO C, LU F
  • 专利权人:   JIANGSU JIANGSHANHONG CHEM FIBER CO LTD, JIANGSU JIANGNAN XIYUAN GRAPHENE TECHNOLOGY CO LTD
  • 国际专利分类:   C08G059/44, C08G069/26, C08G069/28, C08K003/04
  • 专利详细信息:   CN110204707-A 06 Sep 2019 C08G-069/28 201977 Pages: 6 Chinese
  • 申请详细信息:   CN110204707-A CN10450714 28 May 2019
  • 优先权号:   CN10450714

▎ 摘  要

NOVELTY - Preparing graphene in-situ polymerization modified polyamide epoxy curing agent involves adding a dibasic acid and graphene to a reactor. The molar ratio is dibasic acid: graphene is 0.99: 0.01-0.7: 0.3, and the temperature is raised to 160-190 degrees C while stirring, thermostating and sonicating for 2-4 hours, adding the polyamine to the reaction vessel in a ratio of a molar ratio of the dibasic acid and the graphene to the polyamine of 1:1.5-1:3. The reaction is carried out at 150-220 degrees C for 1-4 hours after the addition is completed, to obtain a graphene in-situ polymerization modified polyamide. USE - Method for preparing graphene in-situ polymerization modified polyamide epoxy curing agent. ADVANTAGE - The method enables to prepare graphene in-situ polymerization modified polyamide epoxy curing agent has good physical property, has high heat conduction, has high electric conductivity, has excellent performance with high intensity, has good toughness, has low thermal expansion coefficient, and has improves performance of polymer-based composite material.