• 专利标题:   Manufacture of structure-controllable three-dimensional graphene porous material involves preparing porous metal structure, heating, cooling, performing sand blasting, growing graphene film, washing and drying.
  • 专利号:   WO2016101436-A1, CN105776186-A, US2017267533-A1, JP2018505118-W, CN105776186-B, JP6518765-B2, US10378113-B2
  • 发明人:   SHI Y, YAN C, ZHU W
  • 专利权人:   UNIV HUAZHONG SCI TECHNOLOGY, UNIV HUAZHONG SCI TECHNOLOGY, UNIV HUAZHONG SCI TECHNOLOGY, UNIV HUAZHONG SCI TECHNOLOGY
  • 国际专利分类:   C01B031/04, B33Y010/00, C23F004/04, B22F003/105, B22F003/16, B33Y040/00, C01B032/186, C01B032/184, C01B032/194
  • 专利详细信息:   WO2016101436-A1 30 Jun 2016 C01B-031/04 201649 Pages: 18 Chinese
  • 申请详细信息:   WO2016101436-A1 WOCN075960 07 Apr 2015
  • 优先权号:   CN10826636

▎ 摘  要

NOVELTY - Manufacture of structure-controllable three-dimensional graphene porous material involves constructing (AA) a CAD mold having a three-dimensional porous structure, preparing porous metal structure having corresponding shape by additive manufacturing technique, heating at 900-1500?C under protective atmosphere of an inert gas for 4-24 hours, cooling to room temperature, performing sand blasting and ultrasonic washing to obtain a metal template (BB), growing a graphene film (CC), preparing etching agent, dissolving the metal template by fluxing at 60-90 degrees C, washing and drying. USE - Manufacture of structure-controllable three-dimensional graphene porous material (claimed). ADVANTAGE - The three-dimensional graphene porous material having precise shape is produced quickly. DETAILED DESCRIPTION - Manufacture of structure-controllable three-dimensional graphene porous material involves constructing a CAD mold having a three-dimensional porous structure, preparing a porous metal structure having corresponding shape by an additive manufacturing technique, heating at 900-1500?C under protective atmosphere of an inert gas for 4-24 hours, cooling to room temperature, performing sand blasting and ultrasonic washing to obtain a metal template, growing a graphene film on the metal template by chemical vapor deposition method, preparing 1-3 mol/L etching agent, dissolving the metal template by fluxing at 60-90 degrees C, washing and drying. The metal structure is formed using metal powder having average particle diameter of 5-50 mu m and containing nickel, copper, iron and cobalt. DESCRIPTION OF DRAWING(S) - The drawing shows the flowchart of manufacture of three-dimensional graphene porous material. (Drawing includes non-English language text) Construction of mold (AA) Production of metal template (BB) Growing method (CC) Removal of metal template (DD)