• 专利标题:   Mechanical peeling and grading graphene microchip by putting graphite material and surfactant into continuous screw reaction extruder, placing into cylindrical container filled with solvent, ultrasonically processing, and dispersing.
  • 专利号:   CN105523551-A, CN105523551-B
  • 发明人:   CHEN Q, SUN L, YE R, CHEN W
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD
  • 国际专利分类:   C01B031/04, C01B032/19
  • 专利详细信息:   CN105523551-A 27 Apr 2016 C01B-031/04 201646 Pages: 8 English
  • 申请详细信息:   CN105523551-A CN10069948 02 Feb 2016
  • 优先权号:   CN10069948

▎ 摘  要

NOVELTY - Mechanical peeling and grading graphene microchip comprises putting graphite material and surfactant into continuous screw reaction extruder at 60-350 degrees C at pressure of 20-50 MPa to obtain solid product graphene pre-fabricate slag block, placing into cylindrical container filled with solvent, ultrasonically processing for 30-60 minutes, uniformly dispersing, centrifugally treating for 30-60 minutes, cooling, forming cold solvent, adding coagulant, condensing solvent to obtain cylindrical solid mixture, and splitting according to preset unit size. USE - Method for mechanical peeling and grading graphene microchip (claimed). ADVANTAGE - The method is simple and suitable for large scale production, separates different size, uses high efficiency raw material, and reduces cost. DETAILED DESCRIPTION - Mechanical peeling and grading graphene microchip comprises putting graphite material and surfactant into continuous screw reaction extruder at 60-350 degrees C at pressure of 20-50 MPa to obtain solid product graphene pre-fabricate slag block, placing into cylindrical container filled with solvent, ultrasonically processing for 30-60 minutes, uniformly dispersing, centrifugally treating for 30-60 minutes, cooling, forming cold solvent, adding coagulant, condensing solvent to obtain cylindrical solid mixture, splitting according to preset unit size to obtain N cylindrical solid mixture and center cylindrical solid mixture, adding solvent, heating to dissolve to obtain high purity graphene suspension, drying, and removing solvent.