• 专利标题:   Producing graphene material for super capacitor, by mixing coal, nano calcium carbonate and potassium hydroxide, grinding, placing mixture in corundum porcelain boat, placing boat in furnace, heating mixture, grinding, washing, and drying.
  • 专利号:   CN104098091-A, CN104098091-B
  • 发明人:   HE X, ZHANG H
  • 专利权人:   UNIV ANHUI TECHNOLOGY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104098091-A 15 Oct 2014 C01B-031/04 201503 Chinese
  • 申请详细信息:   CN104098091-A CN10374953 31 Jul 2014
  • 优先权号:   CN10374953

▎ 摘  要

NOVELTY - The method comprises mixing coal, nano calcium carbonate and potassium hydroxide, grinding, placing the mixture in a corundum porcelain boat, placing the corundum porcelain boat in a tube furnace, discharging the inert gas from the furnace, maintaining pressure in the tube furnace at atmospheric pressure or negative pressure of -0.05 Mpa to -0.1 Mpa, heating the mixture, removing the resulting product from the furnace, grinding the product, washing the product with distilled water, and drying to obtain a porous super capacitor graphene material. The inert gas is nitrogen or argon. USE - The method is useful for producing a graphene material for a supercapacitor (claimed). ADVANTAGE - The method is capable of simply producing the graphene material with higher capacity and energy density in an economical manner. DETAILED DESCRIPTION - The method comprises mixing coal, nano calcium carbonate and potassium hydroxide, grinding the mixture, placing the mixture in a corundum porcelain boat, placing the corundum porcelain boat in a tube furnace, discharging the inert gas from the furnace, maintaining pressure in the tube furnace at atmospheric pressure or negative pressure of -0.05 Mpa to -0.1 Mpa, heating the mixture at a rate of 5 degrees C/minute to a temperature of 200 degrees C for 0.5 hour, continuously heating the mixture at a heating rate of 5 degrees C/minute to a temperature of 750 degrees C for 1 hour, and again heating the mixture at a heating rate of 5 degrees C/minute to a temperature of 950 degrees C for 1 hour, removing the resulting product from the furnace, grinding the product, washing the product with distilled water, and drying to obtain a porous super capacitor graphene material. The inert gas is nitrogen or argon.