• 专利标题:   Preparing fluorinated graphene material with adjustable fluorine content comprises e.g. mixing metal salt and fluorinated graphite uniformly, adding mixed product in a tube furnace, and subjecting the reaction product to ultrasonic peeling.
  • 专利号:   CN111620326-A
  • 发明人:   LV J, JIANG L, GUAN X
  • 专利权人:   UNIV FUJIAN JIANGXIA
  • 国际专利分类:   C01B032/10, C01B032/19
  • 专利详细信息:   CN111620326-A 04 Sep 2020 C01B-032/19 202080 Pages: 9 Chinese
  • 申请详细信息:   CN111620326-A CN10344637 27 Apr 2020
  • 优先权号:   CN10344637

▎ 摘  要

NOVELTY - Preparing fluorinated graphene material with adjustable fluorine content comprises (1) mixing the mixed metal salt and fluorinated graphite uniformly, where the mixing method can be grinding or ball milling, (2) adding the mixed product in a tube furnace at 550 degrees C for a period of time, and (3) subjecting the reaction product to ultrasonic peeling in a mixed solution of organic solvent and hydrogen fluoride, separating the upper layer solution by centrifugation, filtering and washing with suction, and vacuum drying to obtain fluorinated graphene. USE - The method is useful for preparing fluorinated graphene material with adjustable fluorine content. ADVANTAGE - The method has low equipment requirements, simple technological process, strong operability, and easy amplification.