• 专利标题:   Preparing amorphous ternary transition metal sulfide/graphene composite material involves adding stannous chloride dihydrate, transition metal salt, and thioacetamide to the graphene oxide dispersion, mixing, and placing them in water bath.
  • 专利号:   CN110611081-A
  • 发明人:   XIA H, FANG L, LIN B, XU J
  • 专利权人:   UNIV NANJING SCI TECHNOLOGY
  • 国际专利分类:   H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN110611081-A 24 Dec 2019 H01M-004/36 202007 Pages: 7 Chinese
  • 申请详细信息:   CN110611081-A CN10618768 15 Jun 2018
  • 优先权号:   CN10618768

▎ 摘  要

NOVELTY - Preparing amorphous ternary transition metal sulfide/graphene composite material involves adding stannous chloride dihydrate, transition metal salt, and thioacetamide to the graphene oxide dispersion, mixing well, and placing them in a water bath at 50-100 degrees C after the reaction, cooling to room temperature after washing with water and ethanol to obtain amorphous ternary transition metal sulfide/graphene composite was obtained after drying, where ratio of stannous chloride dihydrate to graphene oxide is 0.5-5: 30-90 mmol: mg, and ratio of stannous chloride dihydrate to transition metal salt is 1-5: 2-10. USE - Method for preparing amorphous ternary transition metal sulfide/graphene composite material. ADVANTAGE - The method enables to prepare amorphous ternary transition metal sulfide/graphene composite material does not require high-temperature calcination, and can prepare amorphous, non-agglomerated, and high-purity powder materials, has low energy consumption, and in simple manner.