• 专利标题:   Preparing graphene polymer paint involves dissolving graphite in de-ionized water for ultrasonic dispersion to obtain dispersed graphene solution, dissolving to porous material and subjecting to mechanically stirring to obtain paste.
  • 专利号:   CN106987165-A, CN106987165-B
  • 发明人:   CHEN Q, WANG L, ZENG J
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD, HEBEI CHENYANG IND TRADE GROUP CO LTD
  • 国际专利分类:   C09D001/08, C09D133/04, C09D175/04, C09D005/08, C09D007/12, C09D007/61
  • 专利详细信息:   CN106987165-A 28 Jul 2017 C09D-005/08 201773 Pages: 8 Chinese
  • 申请详细信息:   CN106987165-A CN10383147 26 May 2017
  • 优先权号:   CN10383147

▎ 摘  要

NOVELTY - Preparing graphene polymer paint involves dissolving the 20-30 pts. wt. graphite in de-ionized water for ultrasonic dispersion to obtain dispersed graphene solution. The 15-30 pts. wt. porous material is dissolved into dispersed graphene solution at 60-100 degrees C and subjected to mechanically stirring to obtain paste. The obtained product is subjected to spray drying to obtain graphene-porous material. The obtained graphene-porous material is added into the micro-crosslinking reaction kettle which is equipped with thermometer, stirrer and condenser, and added 15-30 pts. wt. polyacrylate emulsion. USE - Method for preparing graphene polymer paint (claimed). ADVANTAGE - The method enables to prepare graphene polymer paint has waterproof film that increases reinforcing and toughening, good corrosion resistance, aging resistance, and high service life. DETAILED DESCRIPTION - Preparing graphene polymer paint involves dissolving the 20-30 pts. wt. graphite in de-ionized water for ultrasonic dispersion to obtain dispersed graphene solution. The 15-30 pts. wt. porous material is dissolved into dispersed graphene solution at 60-100 degrees C and subjected to mechanically stirring to obtain paste. The obtained product is subjected to spray drying to obtain graphene-porous material. The obtained graphene-porous material is added into the micro-crosslinking reaction kettle which is equipped with thermometer, stirrer and condenser, and added 15-30 pts. wt. polyacrylate emulsion. The initiator and sodium hydrogen carbonate are added to obtained mixture and performed the stirring process at room temperature for 1-2 hours. The polyacrylate emulsion-crosslinking film-forming under action of initiator and graphene/porous material are fixed in the micro-pore material. The 0.3-0.5 pts. wt. initiator is polyacrylic ester emulsion. The dosage of sodium hydrogen carbonate is used to adjust pH value to 8-9. The obtained product is adjusted to neutral pH and added 0.5-1 pts. wt. emulsifying agent and 20-30 pts. wt. polyacrylate emulsion under high-speed stirring to disperse and emulsify for 0.5 hours in micelle formation to obtain graphene polymer paint.