• 专利标题:   Graphitic carbon nitride (g-C3N4)-bismuth(III) oxide heterojunction photocatalytic degradation and adsorption composite material used in sewage purification comprises sulfur-doped g-C3N4 supported graphene, bismuth nitrate and zinc nitrate.
  • 专利号:   CN111530489-A
  • 发明人:   ZHANG X
  • 专利权人:   ZHANG X
  • 国际专利分类:   B01J027/24, B01J037/03, B01J037/08, C02F001/30, C02F001/72, C02F001/74, C02F101/30, C02F101/34, C02F101/36, C02F101/38
  • 专利详细信息:   CN111530489-A 14 Aug 2020 B01J-027/24 202073 Pages: 11 Chinese
  • 申请详细信息:   CN111530489-A CN10394061 11 May 2020
  • 优先权号:   CN10394061

▎ 摘  要

NOVELTY - Graphitic carbon nitride (g-C3N4)-bismuth(III) oxide (Bi2O3) heterojunction photocatalytic degradation and adsorption composite material comprises 24-43 pts. wt. sulfur (S)-doped g-C3N4 supported graphene, 35-45 pts. wt. bismuth(III) nitrate, 0.6-1.2 pts. wt. zinc nitrate, and 22-30 pts. wt. citric acid. USE - The graphitic carbon nitride-bismuth(III) oxide heterojunction photocatalytic degradation and adsorption is used in sewage purification. ADVANTAGE - The graphitic carbon nitride-bismuth(III) oxide heterojunction photocatalytic degradation and adsorption promotes the separation of photo-generated electrons and holes, provides porous graphene with a three-dimensional network structure, has abundant pores and pore structures, and adsorbs small molecules after degradation. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing the g-C3N4-Bi2O3 heterojunction photocatalytic degradation and adsorption composite material, comprising adding 24-43 pts. wt. S-doped g-C3N4 supported graphene, 35-45 pts. wt. bismuth(III) nitrate, and 0.6-1.2 pts. wt. zinc nitrate to the ethylene glycol solvent, after the ultrasonic dispersion is uniform, adding 22-30 pts. wt. citric acid, transferring the solution into the reaction kettle, placing in the heating box of the rotary reaction kettle, heating at 150-180 degrees C, reacting for 10-15 hours, filtering the solution to remove the solvent, washing the solid product with distilled water and ethanol, and fully drying.