• 专利标题:   Preparing boron-doped graphene thin film used in e.g. electrochemical capacitor as electrode sheet, by heating substrate and filling with e.g. inert gas, adding substrate to iron chloride solution, and filtering and drying product.
  • 专利号:   CN103779571-A
  • 发明人:   WANG Y, YUAN X, ZHONG H, ZHOU M
  • 专利权人:   OCEAN S KING LIGHTING SCI TECHNOLOGY, SHENZHEN OCEAN S KING LIGHTING SCI, SHENZHEN OCEAN S KING LIGHTING ENG CO
  • 国际专利分类:   H01G009/042, H01M004/133, H01M004/38, H01M004/62
  • 专利详细信息:   CN103779571-A 07 May 2014 H01M-004/62 201444 Pages: 6 Chinese
  • 申请详细信息:   CN103779571-A CN10412159 25 Oct 2012
  • 优先权号:   CN10412159

▎ 摘  要

NOVELTY - Method for preparing boron-doped graphene thin film involves heating the substrate in oxygen-free reaction room and filling with carbon source, boron source gas and inert gas, reacting the mixture, stopping inflating, and adding the substrate to iron(III) chloride solution, filtering the reacted mixture to obtain boron-doped graphene, performing ultrasonic dispersion on the boron-doped graphene using methyl pyrrolidone, filtering the boron-doped graphene suspension, obtaining the solid product in the upper filter film, and drying the solid product. USE - The method is useful for preparing boron-doped graphene thin film which is used in electrochemical capacitor or lithium ion battery as electrode sheet (all claimed). ADVANTAGE - The method enables to prepare boron-doped graphene thin film which has excellent stretching strength and can be directly used as electrode sheet. DETAILED DESCRIPTION - Method for preparing boron-doped graphene thin film involves heating the substrate in oxygen-free reaction room at 500-1300 degrees C and filling with carbon source, boron source gas and inert gas, reacting the mixture at 30-300 degrees C, stopping inflating, and adding the substrate to iron(III) chloride solution, until the substrate is dissolved completely filtering the reacted mixture to obtain boron-doped graphene, performing ultrasonic dispersion on the boron-doped graphene using methyl pyrrolidone, optionally filtering the boron-doped graphene suspension, obtaining the solid product in the upper filter film, and drying the solid product. An INDEPENDENT CLAIM is included for preparing boron-doped graphene thin film which is prepared by the above-mentioned method.