• 专利标题:   Preparation of stable colloidal graphene dispersion liquid, e.g. used for nano-electronics, by mixing graphite with oxidant, reacting with reducing agent, dissolving in substituted naphthalene in organic solvent, centrifuging, and washing.
  • 专利号:   CN103935995-A, CN103935995-B
  • 发明人:   HUANG J, LI H, LIU Z, CHEN X, XIE J
  • 专利权人:   UNIV WUHAN TECHNOLOGY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103935995-A 23 Jul 2014 C01B-031/04 201468 Pages: 11 Chinese
  • 申请详细信息:   CN103935995-A CN10184134 04 May 2014
  • 优先权号:   CN10184134

▎ 摘  要

NOVELTY - Preparation of a stable colloidal graphene dispersion liquid comprises mixing graphite raw material with an oxidant, and ultrasonically centrifuging to obtain a stable graphene oxide; under an in alkaline condition at a pH of 10-11, reacting with a reducing agent for 2-4 hours to obtain graphene; and dispersing the graphene by dissolving in a substituted naphthalene with a different hydrophilic radical in organic solvent, ultrasonically centrifuging, and washing, where the stable colloidal graphene dispersion liquid has a concentration of 0.21-0.25 mg/mL. USE - Method for the preparation of a stable colloidal graphene dispersion liquid (claimed) used for nano-electronics, sensor, compound, cell, super capacitor, and hydrogen storage material. ADVANTAGE - The method is simple and easy, does not use a special device, and is inexpensive.