• 专利标题:   Preparation of multi-hole graphene includes preparing aqueous graphene solution, adding transition metal oxide and concentrated sulfuric acid, reacting, filtering, drying residue, adding acid solution, stirring, filtering, and drying.
  • 专利号:   CN104211052-A, CN104211052-B
  • 发明人:   HUANG J, LI T, LI X, ZHANG X, ZHONG Q
  • 专利权人:   UNIV CHONGQING
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104211052-A 17 Dec 2014 C01B-031/04 201510 Pages: 7 Chinese
  • 申请详细信息:   CN104211052-A CN10444304 28 Aug 2014
  • 优先权号:   CN10444304

▎ 摘  要

NOVELTY - Preparation of multi-hole graphene comprises preparing 1-5 mg/mL aqueous graphene solution using graphene powder as solute and deionized water as solvent; adding transition metal oxide and stirring to obtain first mixture; adding concentrated sulfuric acid and stirring; reacting at 40-90 degrees C for 2-5 hours; vacuum filtering; and drying residue at 60-80 degrees C for 6-12 hours to obtain nano graphene metal oxide; and mixing acid and deionized water, adding product in first step, stirring at 40-90 degrees C for 1-3 hours, filtering, and drying at 60-80 degrees C for 4-12 hours. USE - Method for preparing multi-hole graphene (claimed). DETAILED DESCRIPTION - Preparation of multi-hole graphene comprises: (A) preparing 1-5 mg/mL aqueous graphene solution using graphene powder as solute and deionized water as solvent; adding transition metal oxide and stirring to obtain first mixture, where mass ratio of transition metal oxide to graphene is 1-20:1; adding concentrated sulfuric acid and stirring, where volume ratio of concentrated sulfuric acid and first mixture is 1-4:100; reacting at 40-90 degrees C for 2-5 hours; vacuum filtering; and drying residue at 60-80 degrees C for 6-12 hours to obtain nano graphene metal oxide; and (B) mixing acid and deionized water at ratio of 50:100, adding product in first step, and stirring at 40-90 degrees C for 1-3 hours, where mass-volume ratio of nano graphene metal oxide to acid solution is 1-5:100; filtering; and drying at 60-80 degrees C for 4-12 hours.