• 专利标题:   Method for preparing graphene, involves mixing pyridine and formic acid to obtain mixed solvent, dispersing oxidized graphite in mixed solvent, adding methyl silicone oil, carrying out reflux reaction, isolating and purifying.
  • 专利号:   CN106800290-A
  • 发明人:   CHOU X, LIU Z
  • 专利权人:   HENGYANG JUNJIE CHEM CO LTD
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN106800290-A 06 Jun 2017 C01B-032/184 201747 Pages: 4 Chinese
  • 申请详细信息:   CN106800290-A CN10831956 25 Nov 2015
  • 优先权号:   CN10831956

▎ 摘  要

NOVELTY - The method for preparing graphene, involves (S1) mixing pyridine and formic acid in ratio of 1:1-1:5 to obtain mixed solvent, (S2) dispersing oxidized graphite in mixed solvent to obtain mixed solution, (S3) ultrasonically dispersing mixed solution for 30-40 minutes, (S4) adding 0.2-0.5 ml methyl silicone oil, carrying out reflux reaction at atmospheric pressure, until the black material is not precipitated, stopping reflow reaction, and (S5) isolating the product and purifying to obtain graphene. The addition amount of oxidized graphite to mixed solvent is 5-7 mg/mL. USE - Method for preparing graphene (claimed). ADVANTAGE - The method enables preparation of graphene improved reduction degree of oxidized graphite and improved quality.