• 专利标题:   Preparation of iron-nickel alloy nano-cluster-graphene composite material used for absorbing electromagnetic waves, involves adding graphite oxide and dispersing in organic solvent and adding ferric acetylacetonate and octadecylamine.
  • 专利号:   CN105817648-A, CN105817648-B
  • 发明人:   MA S, MA T, YANG Y, SUN G
  • 专利权人:   UNIV BEIJING NORMAL SCI PARK CO LTD, UNIV BEIJING NORMAL, UNIV BEIJING NORMAL SCI PARK CO LTD
  • 国际专利分类:   B22F009/30, B82Y040/00, C09K003/00
  • 专利详细信息:   CN105817648-A 03 Aug 2016 B22F-009/30 201663 Pages: 15 Chinese
  • 申请详细信息:   CN105817648-A CN10284568 29 Apr 2016
  • 优先权号:   CN10284568

▎ 摘  要

NOVELTY - The preparation of iron-nickel alloy nano-cluster-graphene composite material, involves adding graphite oxide and dispersing in organic solvent (I), adding ferric acetylacetonate, nickel acetylacetonate and octadecylamine, heating the mixture at 100-150 degrees C in the presence of an inert protective gas, maintaining for 20-50 minutes, heating to the boiling reflux, maintaining for 1-5 hours, adding organic solvent (II), stopping reaction, separating reaction products, washing and drying the reaction product. USE - Preparation of iron-nickel alloy nano-cluster-graphene composite material used for absorbing electromagnetic waves (all claimed). ADVANTAGE - The method enables preparation of iron-nickel alloy nano-cluster-graphene composite material with high absorbing properties, and protects and disperses the iron-nickel alloy nano particles. DETAILED DESCRIPTION - The preparation of iron-nickel alloy nano-cluster-graphene composite material, involves adding graphite oxide and dispersing in organic solvent (I), adding ferric acetylacetonate, nickel acetylacetonate and octadecylamine, heating the mixture at 100-150 degrees C in the presence of an inert protective gas, maintaining for 20-50 minutes, heating to the boiling reflux, maintaining for 1-5 hours, adding organic solvent (II), stopping reaction, separating reaction products, washing and drying the reaction product. The mass ratio of graphite oxide and iron acetylacetonate is 0.2-0.3. The mass ratio of graphite oxide and nickel acetylacetonate is 0.1-0.2. The graphite oxide and octadecylamine is 1:80-1:40. INDEPENDENT CLAIMS are included for the following: (1) iron-nickel alloy nano-cluster-graphene composite material; and (2) usage of iron-nickel alloy nano-cluster-graphene composite material for absorbing electromagnetic waves.