• 专利标题:   Preparation of graphene involves inserting graphite rod as cathode and molybdenum rod as anode in electrolytic solution, applying voltage, leaving still, filtering electrolyte solution, drying, and irradiating solid product with laser.
  • 专利号:   CN103964418-A, CN103964418-B
  • 发明人:   LIU D, WANG Y, ZHONG H, ZHOU M
  • 专利权人:   OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING ENG CO LTD, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103964418-A 06 Aug 2014 C01B-031/04 201469 Pages: 7 Chinese
  • 申请详细信息:   CN103964418-A CN10038908 31 Jan 2013
  • 优先权号:   CN10038908

▎ 摘  要

NOVELTY - Preparation of graphene involves inserting graphite rod as cathode and molybdenum rod as anode in an electrolytic solution, applying voltage of 0.8-1.5 V, leaving still for 1-5 minutes, applying voltage of 10-15 V for 4-15 minutes, filtering electrolyte solution, drying, placing solid product under inert gas atmosphere and irradiating with laser of (4-7.5)x 1014 Hz. USE - Preparation of graphene (claimed). ADVANTAGE - The method efficiently and economically provides graphene having high specific surface area, with high productivity, by simple method with reduced consumption of energy.