• 专利标题:   Preparing graphene oxide-trichloroisocyanuric acid composite as disinfectant by dispersing graphene oxide dispersion in N,N-dimethylformamide, adding trichloroisocyanuric acid, centrifuging, dispersing lower solid in water and freeze-drying.
  • 专利号:   CN112369422-A, CN112369422-B
  • 发明人:   JIANG L, YU H, XU S, CUI Q, CHEN Z
  • 专利权人:   UNIV LANZHOU TECHNOLOGY
  • 国际专利分类:   A01N043/66, A01N059/00, A01P001/00, A01P003/00, C01B032/198
  • 专利详细信息:   CN112369422-A 19 Feb 2021 A01N-043/66 202123 Pages: 11 Chinese
  • 申请详细信息:   CN112369422-A CN11278141 16 Nov 2020
  • 优先权号:   CN11278141

▎ 摘  要

NOVELTY - Method for preparing a graphene oxide-trichloroisocyanuric acid composite, involves (a) preparing graphene oxide powder by improved Hummers method, (b) dispersing the graphene oxide dispersion in N,N-dimethylformamide, and ultrasonically treating, (c) adding trichloroisocyanuric acid, 4-dimethylaminopyridine and dicyclohexylcarbodiimide to the mixture obtained in step (b), magnetically stirring at 55-65 degrees C for 1-3 hours, centrifuging, discarding the supernatant, and leaving still to obtain a solid layer, (d) dispersing the lower solid obtained in step (c) in deionized water, adding trichloroisocyanuric acid, and magnetically stirring at 45-55 degrees C for 5-7 hours, (e) washing the product obtained in step (e) with deionized water by vacuum filtration, and (f) pre-freezing the product obtained in step (e) at low temperature, freeze-drying, and grinding to obtain the product. USE - The method is useful for preparing a graphene oxide-trichloroisocyanuric acid composite, which is useful as a disinfectant (all claimed). ADVANTAGE - The composite increases the bactericidal effect of trichloroisocyanuric acid, and exhibits synergistic effect. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the graphene oxide-trichloroisocyanuric acid composite prepared by the method.