• 专利标题:   Preparing high-performance rubber/graphene oxide composite material comprises e.g. heating sulfur to melt, adding vinyl monomer, stirring, dissolving reactant in tetrahydrofuran, filtering, placing mixed rubber into open mill and adding vulcanizing bag, and adding mixed rubber.
  • 专利号:   CN114426707-A, CN114426707-B
  • 发明人:   WANG F, MA Y, WU C, TANG Z, XIAO C, GUO B
  • 专利权人:   SHANDONG LINGLONG TIRE CO LTD, UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   C08K003/04, C08K003/06, C08L007/00, C08L081/04
  • 专利详细信息:   CN114426707-A 03 May 2022 C08L-007/00 202266 Chinese
  • 申请详细信息:   CN114426707-A CN10056310 18 Jan 2022
  • 优先权号:   CN10056310

▎ 摘  要

NOVELTY - Preparing high-performance rubber/graphene oxide composite material comprises (i) heating 50-70% sulfur to 119-160degrees Celsius to melt, adding 0-30% vinyl monomer, stirring for 0-8 hours, adding 20-50% mono-substituted aniline under argon protection, and stirring for 1-4 hours, (ii) dissolving reactant in tetrahydrofuran, filtering to remove unreacted sulfur, pouring the filtered solution into ethanol to obtain purified amino-containing polysulfide, (iii) mixing prepared raw rubber, graphene oxide masterbatch, antioxidant and 1-20 wt.% amino-containing polysulfide according to the mass ratio of raw rubber and graphene oxide masterbatch is 100:26.25-150 in an internal mixer for one stage at 100-170degrees Celsius for 3-10 minutes to obtain a mixed rubber, and (iv) placing mixed rubber into open mill and adding vulcanizing bag, adding mixed rubber, placing for 24-48 hours, and preparing a high-performance rubber/graphene oxide composite material by hot pressing vulcanization. USE - The method is useful for preparing high-performance rubber/graphene oxide composite material. ADVANTAGE - The composite material obviously improves tensile strength and the fixed elongation stress of the rubber/oxidized graphene composite material. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for rubber/graphene oxide composite material prepared by the above mentioned method. DESCRIPTION OF DRAWING(S) - The drawing shows a flow chart of the method for preparing high-performance rubber/graphene oxide composite material (Drawing includes non-English language text).