• 专利标题:   Production of graphene-based pearlescent pigment involves preparing graphene oxide solution and pearlescent pigment dispersion, mixing metal reducing agent, heating, stirring, solid-liquid separating, and drying.
  • 专利号:   CN113214679-A
  • 发明人:   FU Z
  • 专利权人:   HENAN LINGBAO NEW MATERIALS TECHNOLOGY
  • 国际专利分类:   C09C001/00, C09C003/06, C09C003/10, C09B067/00, C01B032/198
  • 专利详细信息:   CN113214679-A 06 Aug 2021 C09C-001/00 202188 Pages: 11 Chinese
  • 申请详细信息:   CN113214679-A CN10502265 08 May 2021
  • 优先权号:   CN10502265

▎ 摘  要

NOVELTY - Production of graphene-based pearlescent pigment comprises adding concentrated sulfuric acid and graphite into a first reaction kettle, mixing, pumping into second reaction kettle, adding methyl ferrate powder in batches, mixing, stirring, injecting purified water or organic solvent, and high-speed shear stirring to form graphene oxide solution; adding weighed water-soluble titanium salt into deionized water, stirring to obtain a titanium salt aqueous solution, adding mica and silica to titanium salt aqueous solution, stirring, adding weighed polyacrylamide, stirring, dropping inorganic acid, stirring, solid-liquid separating, drying, mixing with polyacrylamide and water, stirring, mixing with graphene oxide solution, heating, and stirring; and weighing graphene oxide solution, pearlescent pigment dispersion and metal reducing agent at mass ratio of (40-100):(6-8):1, heating, stirring at 20-80 degrees C for 30 minutes to 24 hours, solid-liquid separating, and drying at 180-200 degrees C. USE - The method is used for producing graphene-based pearlescent pigment.