• 专利标题:   Catalytic synthesis of three-dimensional graphene-like structural carbon material involves reacting ethyl cellulose and sodium hydroxide, mixing with nickel(II) acetate, carbonizing, immersing in hydrochloric acid solution, and drying.
  • 专利号:   CN108249421-A
  • 发明人:   YIN L, ZHANG H, ZHANG F, CHENG R, FANG J, LIN Y
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   B82Y040/00, C01B032/15
  • 专利详细信息:   CN108249421-A 06 Jul 2018 C01B-032/15 201852 Pages: 7 Chinese
  • 申请详细信息:   CN108249421-A CN10205652 13 Mar 2018
  • 优先权号:   CN10205652

▎ 摘  要

NOVELTY - Catalytic synthesis of three-dimensional graphene-like structural carbon material comprises dissolving ethyl cellulose and sodium hydroxide in water at 1:1-3 molar ratio, transferring suspension to PTFE reactor, reacting at 80-120 degrees C for 12 hours, mixing reaction product with nickel(II) acetate at 100:5-20 mass ratio, carbonizing mixture at 700-1000 degrees C for 1-3 hours under argon atmosphere, washing carbonized product with deionized water, suction-filtering, drying, immersing in hydrochloric acid solution to remove residual nickel element, suction-filtering, washing residue until pH of washing solution is 6.5-7.2, and drying at 60 degrees C. USE - Method for catalytic synthesis of three-dimensional graphene-like structural carbon material.