• 专利标题:   Preparing conductive three dimensional printed graphene composite material has dissolving high molecular polymer in organic solvent, adding graphite powder, peeling graphite in dispersion liquid, centrifuging, adding flocculating agent, filtering, washing, drying, grinding and extruding particles.
  • 专利号:   CN113683858-A
  • 发明人:   JI J, SHEN S, LU J, LIU W, LV B, ZHANG Z
  • 专利权人:   UNIV ZHEJIANG TECHNOLOGY
  • 国际专利分类:   B33Y070/10, C01B032/19, C08K003/04, C08L029/04, C08L055/02, C08L067/04, C08L075/04
  • 专利详细信息:   CN113683858-A 23 Nov 2021 C08L-055/02 202238 Chinese
  • 申请详细信息:   CN113683858-A CN10789033 13 Jul 2021
  • 优先权号:   CN10789033

▎ 摘  要

NOVELTY - Preparing conductive three dimensional printed graphene composite material comprises (a) dissolving high molecular polymer in an organic solvent, adding graphite powder to obtain a raw material dispersion, (b) peeling the graphite in the raw material dispersion obtained in step (a) using gas-driven liquid phase stripping method, obtaining dispersion liquid containing high molecular polymer, graphene and graphite powder, (c) placing the dispersion liquid obtained in step (b) into a centrifuge, centrifuging to remove un-stripped graphite powder to obtain a polymer/graphene dispersion liquid, (d) adding flocculating agent in the high molecular polymer/graphene dispersion liquid obtained in step (c), filtering, washing, drying to obtain high molecular polymer/graphene composite particle and (e) grinding and extruding the composite particles obtained in step (d) to obtain graphene composite lines for three dimensional printing. USE - The method is useful for preparing conductive three-dimensional printed graphene composite material. ADVANTAGE - The material has high mechanical strength, high thermal stability and has broad application prospects in three-dimensional printing. The method ensures that the high molecular polymers promote the stripping of graphite; obtains high-quality graphene with complete lattice, small sheet thickness, large and uniform lateral size; improves the composite effect of polymer and graphene; has mild operating conditions, simple process, low device requirements, easy large-scale production and has good industrialization prospect. DESCRIPTION OF DRAWING(S) - The drawing shows a process flow diagram of the preparation method of conductive three dimensional printed graphene composite material (Drawing includes non-English language text).