• 专利标题:   Continuous batch synthesis of single atomic catalyst comprises synthesis of first-step single-atom catalyst precursor by adding metal precursor into solvent and introducing solution into micro-nano-scale atomization devices, spraying metal precursor solution on surface and performing calcination.
  • 专利号:   CN113634288-A, CN113634288-B
  • 发明人:   HE Q, HE X, ZHANG H, JI H
  • 专利权人:   UNIV SUN YATSEN
  • 国际专利分类:   B01J023/72, B01J023/75, B01J023/89, B01J027/24, B01J035/00, B01J037/02, B01J037/08
  • 专利详细信息:   CN113634288-A 12 Nov 2021 B01J-037/08 202223 Chinese
  • 申请详细信息:   CN113634288-A CN10931138 13 Aug 2021
  • 优先权号:   CN10931138

▎ 摘  要

NOVELTY - Continuous batch synthesis of a single atomic catalyst comprises synthesis of first-step single-atom catalyst precursor by adding a metal precursor into a solvent to be configured into 0.01-2 mol/l solution, and then introducing the solution into a plurality of micro-nano-scale atomization devices, (2) uniformly spraying the metal precursor solution on the surface of the carrier material through the micro-nano-scale atomization device, and the metal precursor solution is uniformly sprayed on the surface of the carrier material through micro-nano-scale atomization device, and the carrier material is kept in a dry state in the preparation process through irradiation of the infrared lamp, and then the single-atom catalyst precursor continuously falls into a sample collection groove at the tail end of the conveying device, second step calcination by collecting monatomic catalyst precursor is calcined, and the single-atom catalyst can be obtained after cooling to room temperature. USE - The method is useful for continuous batch synthesis of a single atomic catalyst. ADVANTAGE - The method is suitable for material science and engineering technology field.