• 专利标题:   Method for preparing nano-vanadium nitride/graphene composite paste electrode sensor, involves adding deionized water and concentrated sulfuric acid, further adding graphene oxide and washing with deionized water without sulfate.
  • 专利号:   CN108918609-A
  • 发明人:   LI H, ZHAI Y, LI Z
  • 专利权人:   UNIV JINAN
  • 国际专利分类:   B82Y030/00, G01N027/30
  • 专利详细信息:   CN108918609-A 30 Nov 2018 G01N-027/30 201903 Pages: 6 Chinese
  • 申请详细信息:   CN108918609-A CN10454220 14 May 2018
  • 优先权号:   CN10454220

▎ 摘  要

NOVELTY - A nano-vanadium nitride/graphene composite paste electrode sensor preparing method involves adding 70-75% deionized water and 8-12% concentrated sulfuric acid, mixing well and cooling to room temperature, adding 15-20% graphene oxide and the sum of the components is 100%, soaking at room temperature for 15-18 hours, solid-liquid separation, washing with deionized water without sulfate, drying, grinding to powder and pretreating graphene oxide, adding 42-45% nano-vanadium nitride, 20-25% pre-treated graphene oxide, 12-18% N-ethyl-3-methylpyridine hexafluorophosphate, 8-12% liquid paraffin, 6-10% petroleum ether and the sum of the components is 100% and the grinding is uniform to obtain the nano-vanadium nitride/graphene/N-ethyl-3-methylpyridine hexafluorophosphate mixture carbon paste, placing carbon paste in a glass tube, compacting, drying, polishing with metallographic sandpaper, polishing, and washing with deionized water to obtain the finished product. USE - Method for preparing nano-vanadium nitride/graphene composite paste electrode sensor. ADVANTAGE - The method enables preparing nano-vanadium nitride/graphene composite paste electrode sensor with high sensitivity and better selectivity, in simple and cost effective manner. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a nano-vanadium nitride/graphene composite paste electrode sensor is prepared by the method.