• 专利标题:   Obtaining graphene/iron(II) chromate composite, by sonicating graphene oxide in ethanol, adding iron nitrate, chromium nitrate and aqueous ammonia, pressurizing, subjecting resulting product to annealing process, drying and rinsing.
  • 专利号:   PL427397-A1
  • 发明人:   JEDRZEJEWSKA A, SIBERA D, JEDRZEJEWSKI R
  • 专利权人:   UNIV ZACHODNIOPOMORSKI TECHNOLOGICZNY
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B032/182, C08K003/04, C08K003/22
  • 专利详细信息:   PL427397-A1 20 Apr 2020 C08K-003/04 202042 Pages: 1
  • 申请详细信息:   PL427397-A1 PL427397 15 Oct 2018
  • 优先权号:   PL427397

▎ 摘  要

NOVELTY - Method for obtaining the graphene/iron(II) chromate composite, involves sonicating 0.5 g graphene oxide in 50 ml ethanol, adding iron nitrate and chromium nitrate in a ratio of 1:1 to the solution, adding 25% aqueous ammonia solution, pressurizing the mixture in a solvothermal microwave reactor for 15-45 minutes at a pressure of 4-6 MPa, subjecting the resulting product to an annealing process in an inert atmosphere at a temperature of 500-650 degrees C, and drying and rinsing with distilled water, where the mixture is subjected to pressure treatment in an autoclave at a temperature of 120-200 degrees C for 12-20 hours. USE - The method is used for obtaining the graphene/iron(II) chromate composite.