• 专利标题:   Preparation of graphene/tin oxide composite gas-sensitive material involves taking stannous chloride hydrate, adding surfactant, adding absolute ethanol, mechanically stirring and placing in reaction kettle for solvent heating.
  • 专利号:   CN110498405-A
  • 发明人:   JIANG L, DONG W
  • 专利权人:   NANJING BEIGE ELECTRONIC TECHNOLOGY CO
  • 国际专利分类:   C01B032/182, C01G019/02, G01N027/12
  • 专利详细信息:   CN110498405-A 26 Nov 2019 C01B-032/182 201998 Pages: 9 Chinese
  • 申请详细信息:   CN110498405-A CN10774281 21 Aug 2019
  • 优先权号:   CN10774281

▎ 摘  要

NOVELTY - Preparation of graphene/tin oxide composite gas-sensitive material comprises taking 0.2 mol/L stannous chloride hydrate, adding surfactant with molar ratio of 1-2%, adding 25-35 vol.% absolute ethanol, mechanically stirring for 10-30 minutes, placing in reaction kettle for solvent heating, adding graphene with molar ratio of 0.5-2%, heating at 140-180 degrees C, performing hydrothermal reaction, carrying out ultrasonic assisted reaction for 8-12 hours, collecting milky yellow precipitate at the bottom of reaction kettle by centrifugation, washing with deionized water and absolute ethanol, placing sample in vacuum drying box at 50 degrees C for 7 hours and annealing. USE - The method is used for preparing graphene/tin oxide composite gas-sensitive material. ADVANTAGE - The product has reduced energy consumption and wear and improved service life.