• 专利标题:   Preparing graphene comprises placing silicon carbide in a graphite crucible, vacuumizing, raising and preserving temperature, evaporating, cooling, crushing, ultrasonic peeling and filtering via centrifugal separation.
  • 专利号:   CN103130212-A
  • 发明人:   LI G, LI W
  • 专利权人:   LI G, LI W
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103130212-A 05 Jun 2013 C01B-031/04 201377 Pages: 9 Chinese
  • 申请详细信息:   CN103130212-A CN10390618 30 Nov 2011
  • 优先权号:   CN10390618

▎ 摘  要

NOVELTY - Preparing graphene comprises placing silicon carbide in a graphite crucible, vacuumizing in a high temperature vacuum furnace by filling certain amount of inert gas into the furnace, raising and preserving the temperature for certain time under a certain growth temperature and pressure conditions, evaporating the silicon atoms in silicon carbide, cooling the composition, crushing the obtained microcrystalline graphite, pouring into a container by adding certain amount of solvent, ultrasonic peeling via an ultrasonic device and filtering via centrifugal separation. USE - The method is useful for preparing graphene (claimed). ADVANTAGE - The method is easy to operate and suitable for industries; and produces graphene with high yield and high quality. DETAILED DESCRIPTION - Preparing graphene comprises (i) placing silicon carbide in a graphite crucible, placing the crucible in a high temperature vacuum furnace, closing the furnace door, vacuumizing and filling certain amount of inert gas into the furnace, raising the temperature and preserving the temperature for certain time under a certain growth temperature and pressure conditions, evaporating the silicon atoms in silicon carbide, cooling the composition to obtain microcrystalline graphite; (ii) crushing the microcrystalline graphite, pouring into a container by adding certain amount of solvent, placing in an ultrasonic device and ultrasonic peeling at certain power for a certain time and filtering via centrifugal separation to obtain graphene aqueous dispersion.