• 专利标题:   Preparing graphene model metal composite material involves adding graphene oxide into distilled water, ultrasonically dispersing uniformly to obtain dispersion liquid, dispersing into liquid nitrogen to freeze and placing into freeze dryer.
  • 专利号:   CN108892126-A
  • 发明人:   MA Z
  • 专利权人:   SUZHOU DEHE YAXIN TEXTILE TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/184, C22C001/10
  • 专利详细信息:   CN108892126-A 27 Nov 2018 C01B-032/184 201911 Pages: 5 Chinese
  • 申请详细信息:   CN108892126-A CN10800752 20 Jul 2018
  • 优先权号:   CN10800752

▎ 摘  要

NOVELTY - Preparing graphene model metal composite material involves adding graphene oxide into distilled water, ultrasonically dispersing uniformly to obtain dispersion liquid, where concentration of graphene oxide solution is 6-10mg/mL, dispersing into liquid nitrogen to freeze to solid, placing into freeze dryer at 1000-1200 kilowatts in vacuum for 8-12 hours for liquid to volatilized completely to obtai graphene oxide porous material. The 5-9 pts. wt. iron chloride, 8-12 pts. wt. manganese nitrate and 7-13 pts. wt. tungsten phosphate are added into 40-50 pts. wt. ethanol, stirring for 10-30 minutes. The 6-10 parts of ethylene-vinyl acetate copolymer is added, stirred continuously and reacted for 30-50 minutes at 80-100 degrees C to obtain mixed solution. The prepared graphene oxide porous material is added in mixed solution u8nder nitrogen atmosphere in tube furnace at 3-5 degrees C/minute. The temperature is reaised to 650-800 degrees C and calcined for 2-4 hours to obtain graphene-metal composite material. USE - Method for preparing graphene model metal composite material.