▎ 摘　　要

NOVELTY - Preparation of molybdenum disulfide/graphene intercalation structure material comprises respectively dissolving molybdenum source and sulfur source in water by fully stirring, obtaining molybdenum source solution and sulfur source solution, adding surfactant into sulfur source solution, stirring uniformly to obtain transparent solution, gradually dripping the transparent solution into molybdenum source solution, fully stirring to obtain mixed liquid, sealing and reacting to obtain reaction product, fully washing the reaction product, drying, and calcining under inert gas condition. USE - Preparation of molybdenum disulfide/graphene intercalation structure material (claimed) used for high-efficiency photocatalyst and energy material. ADVANTAGE - The method is simple, green and environment-friendly, and provides molybdenum disulfide/graphene intercalation structure material, which has expanded layers of molybdenum disulfide. DETAILED DESCRIPTION - Preparation of molybdenum disulfide/graphene intercalation structure material comprises respectively dissolving molybdenum source and sulfur source in water by fully stirring, obtaining molybdenum source solution and sulfur source solution, adding surfactant into sulfur source solution, stirring uniformly to obtain transparent solution, where mol ratio of molybdenum element and sulfur element is 1:2.5-5, gradually dripping the transparent solution into molybdenum source solution, fully stirring to obtain mixed liquid, sealing and reacting at 100-300 degrees C and 120-300 MPa for 3-48 hours to obtain reaction product, fully washing the reaction product, drying, calcining at 600-800 degrees C under inert gas condition for 1-3 hours and obtaining the product.