• 专利标题:   Preparing high-strength and high-temperature-resistant ceramic fiber elastomer thermal insulation material used in elastic aerogel material, involves dispersing uniformly first portion of ceramic microfiber, graphene oxide solution, surfactant and water through first stirring to obtain dispersion.
  • 专利号:   CN115057686-A, CN115057686-B
  • 发明人:   ZHANG H, ZHAO Y, WANG P, HUANG H, LI W, LIU Y, ZHANG W
  • 专利权人:   AEROSPACE RES INST SPECIAL MATERIALS
  • 国际专利分类:   C04B014/46, C04B030/02
  • 专利详细信息:   CN115057686-A 16 Sep 2022 C04B-030/02 202296 Chinese
  • 申请详细信息:   CN115057686-A CN10749815 29 Jun 2022
  • 优先权号:   CN10749815

▎ 摘  要

NOVELTY - Preparing high-strength and high-temperature-resistant ceramic fiber elastomer thermal insulation material involves dispersing uniformly first portion of ceramic microfiber, graphene oxide solution, surfactant and water through the first stirring to obtain a dispersion, adding a reducing agent and a silicone rubber prepolymer to the dispersion, dispersing uniformly through the second stirring, performing pre-reduction reaction to obtain a pre-reduction product, adding a second portion of ceramic microfiber to the pre-reduced product, dispersing uniformly through the third stirring, and performing reduction reaction to obtain ceramic microfiber/graphene composite wet gel. USE - Method for preparing high-strength and high-temperature-resistant ceramic fiber elastomer thermal insulation material used in elastic aerogel material, aerospace high-temperature thermal insulation, and high temperature heat insulation of chemical metallurgy or high temperature heat insulation of nuclear power generation (claimed). ADVANTAGE - The prepared high-strength and high-temperature-resistant ceramic fiber elastomer thermal insulation material has the maximum compression strength of 0.75 megapascal under 10% compression deformation and the long-term temperature resistance of 1300℃. DETAILED DESCRIPTION - Preparing high-strength and high-temperature-resistant ceramic fiber elastomer thermal insulation material involves dispersing uniformly first portion of ceramic microfiber, graphene oxide solution, surfactant and water through the first stirring to obtain a dispersion, adding a reducing agent and a silicone rubber prepolymer to the dispersion, dispersing uniformly through the second stirring, performing pre-reduction reaction to obtain a pre-reduction product, adding a second portion of ceramic microfiber to the pre-reduced product, dispersing uniformly through the third stirring, performing reduction reaction to obtain ceramic microfiber/graphene composite wet gel, soaking the obtained ceramic microfiber/graphene composite wet gel in water, wet-pressing the soaked ceramic microfiber/graphene composite wet gel to obtain wet-pressed ceramic microfiber/graphene composite wet gel, subjecting orderly wet-pressed ceramic microfiber/graphene composite wet gel to the steps of pre-freezing, freezing, drying, and annealing to obtain a high-strength and high-temperature-resistant ceramic fiber elastomer heat insulating material. An INDEPENDENT CLAIM is included for a high-strength and high-temperature-resistant ceramic fiber elastomer thermal insulation material is prepared by preparation method.