• 专利标题:   Preparation of high-capacity graphene aerogel negative electrode material includes weighing lithium titanate precursor powder, adding graphene/carbon nanotube dispersion liquid and performing carbon dioxide supercritical extraction drying.
  • 专利号:   CN110165151-A
  • 发明人:   CHE C
  • 专利权人:   BEIJING OUMEIZHONG SCI TECHNOLOGY RES
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/485, H01M004/587
  • 专利详细信息:   CN110165151-A 23 Aug 2019 H01M-004/36 201977 Pages: 6 Chinese
  • 申请详细信息:   CN110165151-A CN10111999 05 Feb 2018
  • 优先权号:   CN10111999

▎ 摘  要

NOVELTY - Preparation of high-capacity graphene aerogel negative electrode material comprises weighing 30-50 mg lithium titanate precursor powder, adding 200 mL graphene/carbon nanotube dispersion liquid for three times, dispersing for 0.8-1 hours with ultrasonic waves to obtain mixed solution, sealing mixed solution in PTFE high-pressure reaction kettle, reacting at 180-200 degrees C for 10-12 hours, cooling to room temperature to obtain graphene hydrogel/carbon nanotube/lithium titanate, cleaning graphene hydrogel/carbon nanotube/lithium titanate particles with absolute ethyl alcohol, drying graphene hydrogel/carbon nanotube/lithium titanate particles, performing carbon dioxide supercritical extraction drying to obtain graphene aerogel/carbon nanotube/lithium titanate particles and heating graphene aerogel/carbon nanotube/lithium titanate particles at 1000-1200 degrees C for 3-5 hours. USE - The method is for preparation of high-capacity graphene aerogel negative electrode material. ADVANTAGE - The material has good electrochemical performance.