• 专利标题:   Preparing graphene porous film comprises e.g. adding pore-forming agent to graphene oxide solution, dispersing, drying, reducing obtained composite film of graphene oxide and pore-forming agent, then removing pore-forming agent, and drying.
  • 专利号:   CN106395802-A
  • 发明人:   XIN W, ZHAO Z, FENG L
  • 专利权人:   UNIV SHANDONG TECHNOLOGY
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN106395802-A 15 Feb 2017 C01B-032/184 201722 Pages: 6 Chinese
  • 申请详细信息:   CN106395802-A CN10808334 08 Sep 2016
  • 优先权号:   CN10808334

▎ 摘  要

NOVELTY - Preparing graphene porous film comprises e.g. (i) adding graphite oxide into water to obtain graphite oxide dispersion, and carrying out ultrasonic dispersion to obtain graphene oxide solution, (ii) adding pore-forming agent to graphene oxide solution, dispersing pore-forming agent in graphene oxide, sucking, and/or drying to obtain composite film of graphene oxide and pore-forming agent, (iii) reducing composite film of graphene oxide and pore-forming agent, and washing to obtain composite film of graphene and pore-forming agent, and (iv) removing pore-forming agent, and drying. USE - The method is useful for preparing graphene porous film (claimed). ADVANTAGE - The method has high yield, simple preparation process, and produces graphene porous film having pore size of 100-1000 nm. DETAILED DESCRIPTION - Preparing graphene porous film comprises (i) adding graphite oxide into water to obtain graphite oxide dispersion, and carrying out ultrasonic dispersion to obtain graphene oxide solution, (ii) adding pore-forming agent to graphene oxide solution, dispersing pore-forming agent in graphene oxide, sucking, and/or drying to obtain composite film of graphene oxide and pore-forming agent, (iii) reducing composite film of graphene oxide and pore-forming agent, and washing to obtain composite film of graphene and pore-forming agent, and (iv) removing pore-forming agent with organic solvent under wet conditions, and then drying using critical point drying method for 1-5 hours to obtain final product.