• 专利标题:   Preparing graphene modified phenolic resin comprises e.g. pouring graphene powder into N-methylpyrrolidone, performing ultrasonic treatment, heating resulting supernatant, adding graphene nanosheet into phenolic resin and stirring.
  • 专利号:   CN107880483-A
  • 发明人:   HU Y
  • 专利权人:   SUQIAN CHINA SOUTHERN AIRLINES NEW MATER
  • 国际专利分类:   C08K003/04, C08K007/00, C08L061/06
  • 专利详细信息:   CN107880483-A 06 Apr 2018 C08L-061/06 201830 Chinese
  • 申请详细信息:   CN107880483-A CN11169840 17 Nov 2017
  • 优先权号:   CN11169840

▎ 摘  要

NOVELTY - Preparing graphene modified phenolic resin comprises e.g. (i) pouring graphene powder into N-methylpyrrolidone, mixing, performing ultrasonic treatment to obtain graphene solution, then taking supernatant, heating resulting supernatant at 80-150 degrees C for 3-5 hours to obtain solid powder, then washing resulting solid powder with ethanol, then placing at 80-150 degrees C, heating for 3-5 hours to obtain graphene nanosheet, and (ii) adding graphene nanosheet obtained in step (i) into phenolic resin, stirring at high-speed and performing ultrasonic treatment to obtain graphene-modified phenolic resin. USE - The method is useful for preparing graphene modified phenolic resin. ADVANTAGE - The phenolic resin improves heat resistance and toughness. DETAILED DESCRIPTION - Preparing graphene modified phenolic resin comprises (i) pouring graphene powder into N-methylpyrrolidone, mixing and performing ultrasonic treatment to obtain graphene solution, then taking supernatant, allowing to stand for 1-3 hours, heating and treating resulting supernatant at 80-150 degrees C for 3-5 hours to obtain solid powder, then washing resulting solid powder with ethanol, then placing at 80-150 degrees C, heating for 3-5 hours and again washing with ethanol for twice to obtain graphene nanosheet, and (ii) adding graphene nanosheet obtained in step (i) into phenolic resin, stirring at high-speed and performing ultrasonic treatment to obtain graphene-modified phenolic resin.