• 专利标题:   Preparing and purifying nanoparticles of plasma ammoniated graphene-magnetic core structure, comprises placing nanoparticles of graphene-magnetic core structure in processing chamber, carrying out ammonia modification of nanoparticles, and removing non-magnetic free graphene.
  • 专利号:   CN116143110-A
  • 发明人:   LI Y, WANG M, MA Z, WANG Q
  • 专利权人:   UNIV BEIJING TECHNOLOGY
  • 国际专利分类:   C01B032/194, C01B032/196
  • 专利详细信息:   CN116143110-A 23 May 2023 C01B-032/194 202352 Chinese
  • 申请详细信息:   CN116143110-A CN11396943 23 Nov 2021
  • 优先权号:   CN11396943

▎ 摘  要

NOVELTY - Preparing and purifying nanoparticles of plasma ammoniated graphene-magnetic core structure, comprises (a) placing the nanoparticles of graphene-magnetic core structure in the processing chamber, so that the processing gas flows into the processing chamber; (b) using a plasma excitation source to excite the processing gas to form a plasma, and exposing the nanoparticles of the graphene-magnetic core structure to the plasma environment, and carrying out ammonia modification of nanoparticles with graphene-magnetic core structure; (c) mixing the plasma-treated graphene-magnetic core structure nanoparticles with water, subjecting the mixture to high-speed shear dispersion, and carrying out magnetic separation to remove non-magnetic free graphene to obtain magnetic material which is the crude product; and (d) mixing crude product with an aqueous ethanol solution, and subjecting the mixture to high-pressure homogenization and magnetic separation, and removing the non-magnetic free graphene. USE - The method is useful for preparing and purifying nanoparticles of plasma ammoniated graphene-magnetic core structure. ADVANTAGE - The method is simple in process, mild and controllable, high in yield, and can be prepared to obtain high-purity aminated modified nano-graphene of the magnetic core structure. DESCRIPTION OF DRAWING(S) - The drawing shows a flow chart illustrating the method for preparing and purifying nanoparticles of plasma ammoniated graphene-magnetic core structure (Drawing includes non-English language text).