• 专利标题:   Preparation of inorganic mixed smoke-inhibiting flame retardant for preparing flame-retardant epoxy material, involves adding zinc salt and stannate to graphene oxide suspension, hydrothermally reacting, filtering, washing, and drying.
  • 专利号:   CN104893248-A, CN104893248-B
  • 发明人:   LIU X, QU H, XU J, LIU H, QI Y, TANG H
  • 专利权人:   UNIV HEBEI
  • 国际专利分类:   C08K003/04, C08K003/24, C08L063/00
  • 专利详细信息:   CN104893248-A 09 Sep 2015 C08L-063/00 201615 Pages: 12 Chinese
  • 申请详细信息:   CN104893248-A CN10277855 27 May 2015
  • 优先权号:   CN10277855

▎ 摘  要

NOVELTY - Preparation of inorganic mixed smoke-inhibiting flame retardant, involves suspending soluble zinc salt in 0.4-0.6 mg/mL graphene oxide suspension in a concentration of 2.5-9 mmol/L, stirring for 15-20 minutes, adding equimolar soluble stannate, stirring for 30-40 minutes to obtain a precursor solution, hydrothermally reacting the precursor solution at 120-160 degrees C for 6-12 hours, cooling, filtering, water-washing, and drying. USE - Preparation of inorganic mixed smoke-inhibiting flame retardant useful for preparing flame-retardant materials e.g. flame-retardant epoxy resin materials (all claimed). ADVANTAGE - The method enables simple preparation of inorganic mixed smoke-inhibiting flame retardant under easy-to-control reaction conditions with easy scale up. The obtained product has excellent flame retardance effect, and provides epoxy materials having excellent smoke-inhibiting function and flame retardance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for flame-retardant epoxy resin material comprising 76-82 wt.% epoxy resin, 14-16 wt.% curing agent, and 3-9 wt.% flame retardant.