• 专利标题:   Preparation of graphene by adding soluble inorganic salt and/or soluble organic compound and expanded graphite into distilled water, heating, mixing, ball milling, washing, performing suction filtration and drying.
  • 专利号:   CN103058176-A
  • 发明人:   CHEN G, LONG J, ZHAO L
  • 专利权人:   UNIV HUAQIAO, XIAMEN KNANO GRAPHENE TECHNOLOGY CO LTD
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103058176-A 24 Apr 2013 C01B-031/04 201371 Pages: 10 Chinese
  • 申请详细信息:   CN103058176-A CN10593496 29 Dec 2012
  • 优先权号:   CN10593496

▎ 摘  要

NOVELTY - Preparing graphene includes respectively weighing soluble inorganic salt and/or soluble organic compound and expanded graphite; adding the soluble inorganic salt and/or the soluble organic compound and the expanded graphite into distilled water, heating, mixing uniformly, placing into a drying box until the water is volatilized completely to obtain the mixture of the expanded graphite and the inorganic salt and/or the organic compound, ball milling; and separating ball-milling products, washing with distilled water, performing suction filtration and drying to obtain the graphene. USE - Method for preparing graphene (claimed). ADVANTAGE - The method is simple, environment-friendly, and easy to operate, and has no special requirement to the equipment, low cost and high efficiency. DETAILED DESCRIPTION - Preparing graphene comprises: (A) respectively weighing soluble inorganic salt and/or soluble organic compound and expanded graphite according to the mass ratio of the soluble inorganic salt and/or the soluble organic matter to the expanded graphite of 10:1-200:1, where the expanded graphite serves as a raw material; (B) adding the soluble inorganic salt and/or the soluble organic compound and the expanded graphite into distilled water, heating, mixing uniformly until the soluble inorganic salt and/or the soluble organic compound are dissolved completely, placing into a drying box until the water is volatilized completely to obtain the mixture of the expanded graphite and the inorganic salt and/or the organic compound, placing the mixture into a ball-milling tank and performing ball milling; and (C) separating ball-milling products, washing with distilled water for 3-5 times, performing suction filtration and drying to obtain the graphene.