• 专利标题:   Preparing graphene attached plastic loaded gold-cobalt sodium borohydride electro-oxidation catalyst, comprises fixing alkaline-resistant double-sided adhesive tape on one side of plastic surface, and coating graphene on other side.
  • 专利号:   CN104091958-A, CN104091958-B
  • 发明人:   CAO D, WANG G, YAN P, WANG B, ZHANG D, CAI Z
  • 专利权人:   UNIV HARBIN ENGINEERING
  • 国际专利分类:   B01J031/28, H01M004/90
  • 专利详细信息:   CN104091958-A 08 Oct 2014 H01M-004/90 201503 Pages: 5 Chinese
  • 申请详细信息:   CN104091958-A CN10323834 09 Jul 2014
  • 优先权号:   CN10323834

▎ 摘  要

NOVELTY - Preparing graphene attached plastic loaded gold-cobalt sodium borohydride electro-oxidation catalyst, comprises fixing alkaline-resistant double-sided adhesive tape on one side of plastic surface, coating graphene on other side of double-sided adhesive tape, applying compaction pressure on graphene, placing graphene-adhered plastic in aqueous solution (6 g cobalt nitrate and 1 g ammonium chloride), pre-activating at 1 V for 3 minutes, electrically depositing cobalt, placing graphene adhered plastic cobalt substrate in 0.8 mmol/ml gold chloride solution for 3-5 minutes. USE - The method is useful for preparing graphene attached plastic loaded gold-cobalt sodium borohydride electro-oxidation catalyst (claimed). DETAILED DESCRIPTION - Preparing graphene attached plastic loaded gold-cobalt sodium borohydride electro-oxidation catalyst, comprises fixing alkaline-resistant double-sided adhesive tape on one side of plastic surface, coating 10-15 mg.cm/2 graphene on other side of double-sided adhesive tape, applying compaction pressure on graphene at 4-8 MPa, placing graphene-adhered plastic in 1 l aqueous solution (6 g cobalt nitrate and 1 g ammonium chloride), pre-activating at 1 V for 3 minutes, electrically depositing cobalt at 1 V for 0.5-1 hour, placing graphene adhered plastic cobalt substrate in 0.8 mmol/ml gold chloride solution for 3-5 minutes.