• 专利标题:   Preparing high-quality low-defect single layer graphene comprises preparing first-order graphite intercalation compound solution, adding benzonitrile solution, adding solution in cleaned silicon/silicon dioxide surface, coating and drying.
  • 专利号:   CN106430165-A
  • 发明人:   HE D, LU J, TU X, YIN G, JIN C
  • 专利权人:   NAT ENG RES CENT NANOTECHNOLOGY
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN106430165-A 22 Feb 2017 C01B-032/184 201722 Pages: 6 Chinese
  • 申请详细信息:   CN106430165-A CN10948418 26 Oct 2016
  • 优先权号:   CN10948418

▎ 摘  要

NOVELTY - Preparing high-quality low-defect single layer graphene comprises adding dissolving alkali metal potassium in organic solvent dimethyl sulfoxide (DMSO) and/or tetrahydrofuran (THF), to obtain alkali metal-organic solvent insert, adding spherical graphite, sealing, ultrasonically treating, allowing to stand, to form first-order graphite intercalation compound (KC8) solution, adding excess of benzonitrile solution, transferring the insert in the graphite interlayer compound, adding solution in the surface of the cleaned silicon/silicon dioxide surface, spin coating and drying. USE - The method is useful for preparing high-quality low-defect single layer graphene (claimed). ADVANTAGE - The method: reduces the production cost of high-quality single-layer graphene; and improves the production efficiency so that the mass production is possible. DETAILED DESCRIPTION - Preparing high-quality low-defect single layer graphene comprises (a) adding dissolving alkali metal potassium in organic solvent dimethyl sulfoxide (DMSO) and/or tetrahydrofuran (THF), to obtain alkali metal-organic solvent insert, (b) adding spherical graphite, sealing with more than 1000 W power, ultrasonically treating for 30 minutes, allowing to stand for 2 hours, to form first-order graphite intercalation compound (KC8) solution, (c) adding an excess of benzonitrile solution to the first-order graphite intercalation compound solution and transferring the insert in the graphite interlayer compound, (d) adding the solution in a dropwise manner in the surface of the cleaned silicon/silicon dioxide surface, spin coating and drying.