• 专利标题:   Preparing graphene complex manganese lithium phosphate material comprises e.g. dissolving lithium hydroxide in mixed solvent, adding e.g. graphene oxide solution, hydrothermally reacting, mixing glucose and calcining.
  • 专利号:   CN106684368-A, CN106684368-B
  • 发明人:   ZHOU T, WANG B, XIONG W, CHOU R, QIU R
  • 专利权人:   YANCHENG INST TECHNOLOGY, YANCHENG INST TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN106684368-A 17 May 2017 H01M-004/36 201746 Pages: 11 Chinese
  • 申请详细信息:   CN106684368-A CN10082734 16 Feb 2017
  • 优先权号:   CN10082734

▎ 摘  要

NOVELTY - Preparing graphene complex manganese lithium phosphate material comprises dissolving the lithium hydroxide in the mixed solvent, adding manganese sulfate solution and graphene oxide solution, incubating and adding phosphoric acid solution, subjecting to magnetic stirring, transferring the mixed solution to a reaction vessel for the first hydrothermal reaction, cooling, heating for a second hydrothermal reaction, mixing the solid precursor with glucose and calcining in an inert gas atmosphere. USE - The method is useful for preparing graphene complex manganese lithium phosphate material (claimed). ADVANTAGE - The method: improves the performance of the product; is simple; and can be produced in batch. The material has high product performance. DETAILED DESCRIPTION - Preparing graphene complex manganese lithium phosphate material comprises dissolving the lithium hydroxide in the mixed solvent, adding manganese sulfate solution and graphene oxide solution, to obtain the first solution, ultrasonically stirring, incubating and adding phosphoric acid solution to the first solution for multiple times, to obtain a mixed solution, subjecting the mixed solution to magnetic stirring, transferring the mixed solution to a reaction vessel for the first hydrothermal reaction, cooling the mixture after completion of the reaction, heating for a second hydrothermal reaction, to obtain a solid precursor, mixing the solid precursor with glucose and calcining in an inert gas atmosphere. An INDEPENDENT CLAIM is also included for graphene complex manganese lithium phosphate material prepared by above method.