• 专利标题:   Preparing hollow, porous, multi-level polyacrylonitrile-based carbon fiber to adsorption, catalysis, filtering, electric and heat energy storage material, involves forming cortex/core spinning liquid by coaxial/skin-core wet spinning to form skin-core structure filaments.
  • 专利号:   CN115948821-A
  • 发明人:   GUO Y, QU Y, CHENG L, SUN J
  • 专利权人:   UNIV JIANGNAN
  • 国际专利分类:   D01D005/34, D01F001/08, D01F001/10, D01F008/08, D01F008/10, D01F009/22
  • 专利详细信息:   CN115948821-A 11 Apr 2023 D01F-009/22 202337 Chinese
  • 申请详细信息:   CN115948821-A CN10153632 21 Feb 2023
  • 优先权号:   CN10153632

▎ 摘  要

NOVELTY - Preparing hollow, porous, multi-level polyacrylonitrile-based carbon fiber involves forming cortex/core spinning liquid by coaxial/skin-core wet spinning to form skin-core structure filaments, drying the skin-core structure thread strips in an oven at 30-80℃ for 180-400 minutes to obtain porous coaxial as-spun fibers, pre-oxidizing the porous coaxial as-spun fibers, heating up to 200-250℃ at a rate of 2℃/minutes, and keeping for 60-180 minutes. The pre-oxidized fiber is heated to 700-900℃ at a rate of 4℃/minutes under the protection of an inert gas, and kept for 60-180 minutes to obtain a product. USE - Method for preparing hollow, porous, multi-level polyacrylonitrile-based carbon fiber used to adsorption, catalysis, filtering, electric and heat energy storage material. ADVANTAGE - The merhod produces product which has excellent thermal stability, mechanical strength, thermal conductivity, and mechanical strength.