• 专利标题:   Preparation of graphene film involves placing high purity soluble salt into corundum boat, putting into CVD tubular furnace, vacuuming, filling inert gas, cleaning cavity, and introducing hydrogen, argon or nitrogen gas.
  • 专利号:   CN108423658-A
  • 发明人:   PENG P, WANG Z, TIAN Z, SONG J, LI M, REN L, FU Y
  • 专利权人:   UNIV PEKING
  • 国际专利分类:   C01B032/186
  • 专利详细信息:   CN108423658-A 21 Aug 2018 C01B-032/186 201865 Pages: 7 Chinese
  • 申请详细信息:   CN108423658-A CN10250018 26 Mar 2018
  • 优先权号:   CN10250018

▎ 摘  要

NOVELTY - A graphene film is prepared by placing high purity soluble salt into corundum boat, putting into CVD tubular furnace, vacuuming, filling inert gas, cleaning cavity, introducing hydrogen, argon or nitrogen gas at flow rate of 1 sccm, heating, melting to form soluble salt solution, introducing gaseous or solid carbon source, or introducing volatile matter, closing tubular furnace power supply, cooling, re-solidifying, obtaining graphene film soluble salt block sample, spin coating, drying, soaking in deionized water, and washing with acetone. USE - Method for preparing graphene film. ADVANTAGE - The method is low-cost, environment-friendly and has little byproducts.