• 专利标题:   Method for preparing cobalt hydroxide/flexible graphene electrode material, involves immersing bacterial cellulose in deionized water, dispersing graphene oxide in water followed by forming slurry, depositing, placing in oven and filtering.
  • 专利号:   CN105374574-A, CN105374574-B
  • 发明人:   LIU R, MA L, YUAN G, ZHANG F, YANG S, LI E
  • 专利权人:   HARBIN INST TECHNOLOGY, HARBIN INST TECHNOLOGY
  • 国际专利分类:   H01G011/22, H01G011/32, H01G011/86
  • 专利详细信息:   CN105374574-A 02 Mar 2016 H01G-011/32 201622 Pages: 9 English
  • 申请详细信息:   CN105374574-A CN10990677 25 Dec 2015
  • 优先权号:   CN10990677

▎ 摘  要

NOVELTY - A cobalt hydroxide/flexible graphene electrode material preparing method involves immersing bacterial cellulose in deionized water, ultrasonic washing the acid, and dispersing in deionized water and transferring to a homogenizer. Graphene oxide is dispersed in distilled water to obtain a graphene oxide dispersion, followed by bacterial cellulose forming a slurry, depositing cobalt hydroxide graphene composite, and placing in oven to obtain cobalt hydroxide/graphene flexible electrode material, cobalt hydroxide/graphene flexible cobalt hydroxide electrode material after vacuum filtration. USE - Method for preparing cobalt hydroxide/flexible graphene electrode material that is utilized as positive electrode material of supercapacitor (claimed). ADVANTAGE - The electrode material has high specific capacitance, better mechanical properties and better capacitive effect. DETAILED DESCRIPTION - A cobalt hydroxide/flexible graphene electrode material preparing method involves immersing bacterial cellulose in deionized water, ultrasonic washing the acid, and dispersing in deionized water and transferring to a homogenizer, high speed stirring to obtain a substrate with a bacterial cellulose pulp. Graphene oxide is dispersed in distilled water to obtain a graphene oxide dispersion, the cobalt salt is dissolved in distilled water, and added to the graphene oxide dispersion, ultrasonic dispersion evenly, aqueous ammonia is added and mixed uniformly, transferred to a reaction vessel and heated to obtain cobalt hydroxide graphene composite, followed by bacterial cellulose forming a slurry by vacuum filtering, depositing cobalt hydroxide graphene composite, and placing in a vacuum oven and drying to obtain cobalt hydroxide/graphene flexible electrode material, cobalt hydroxide/graphene flexible cobalt hydroxide electrode material after vacuum filtration with bacterial cellulose at mass ratio of (0.1-6): 1, where ratio of graphene oxide and cobalt salt is 1mg: (0.001-0.3 mmol), mass volume of graphene oxide and ammonia ratio is 1 mg: (0.001-0.1) mL.