• 专利标题:   Preparing functional nanocomposite hydrogel involves mixing alcohol solution of graphene oxide with acetonitrile to obtain suspension, and adding ammonia-water to suspension at room temperature, stirring, slowly adding alcohol solution.
  • 专利号:   CN108212127-A
  • 发明人:   XU M, ZHANG L, CAO J, XUE C, FANG F, LI C
  • 专利权人:   UNIV HOHAI
  • 国际专利分类:   B01J020/26, B01J020/28, C02F001/28, C02F001/30, C02F001/72, C02F101/30
  • 专利详细信息:   CN108212127-A 29 Jun 2018 B01J-020/26 201853 Pages: 6 Chinese
  • 申请详细信息:   CN108212127-A CN10047197 18 Jan 2018
  • 优先权号:   CN10047197

▎ 摘  要

NOVELTY - Preparing functional nanocomposite hydrogel involves mixing alcohol solution of graphene oxide with acetonitrile to obtain suspension, adding ammonia-water (NH3-H2O) to the suspension at room temperature, stirring, slowly adding alcohol solution of iron acetylacetonate to the obtained solution, stirring, maintaining obtained suspension at 50-80 degrees C for 10-12 hours to pre-grow amorphous iron oxide nanoparticles on the surface of the graphene oxide. The obtained material is washed with ethanol, centrifuged, and the obtained precipitate is redispersed in distilled water to obtain an oxide oxide dispersion. The calcium nitrate, acrylamide monomer, monobromoacetic acid and ammonium persulfate is dissolved in the aforementioned graphene oxide dispersion. The mixture is degassed, placed in a container, and dried in an oven to obtain an iron oxide/graphene oxide/polyacrylamide hydrogel (PAM). USE - Method for preparing functional nanocomposite hydrogel used for degrading organic contaminants, where organic contaminant is an organic dye (claimed). ADVANTAGE - The method enables to prepare functional nanocomposite hydrogel which has high mechanical strength, high photo-Fenton activity and good adsorption performance.