• 专利标题:   Assembling an amine-functionalized graphene by adding sodium borohydride solution to graphene and copper sulfate aqueous solution, washing with distilled water and ethanol, oven-drying, and adding to diethylenetriamine.
  • 专利号:   CN103773086-A, CN103773086-B
  • 发明人:   LIAO Q, ZHANG C, ZHANG W
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   C09C001/46, C09C003/06, C09C003/08
  • 专利详细信息:   CN103773086-A 07 May 2014 C09C-001/46 201444 Pages: 9 Chinese
  • 申请详细信息:   CN103773086-A CN10017604 15 Jan 2014
  • 优先权号:   CN10017604

▎ 摘  要

NOVELTY - Assembling an amine-functionalized graphene comprises preparing an electroless plating solution by sonicating 0.1-1 g graphene and 100 mL copper sulfate aqueous solution for 2 hours; pouring mixture in a copper three-necked flask, adding 100 mL sodium borohydride (NaBH4) solution, and reacting for 0.5-8 hours; washing the copper-modified graphene with distilled water and ethanol for 3 times, and oven-drying at 40 degrees C; and adding nano copper-modified graphene to diethylenetriamine, where the mass ratio of nano copper-modified graphene and diethylenetriamine is 0.005-0.012. USE - Method for assembling an amine-functionalized graphene (claimed). ADVANTAGE - The amine-functionalized graphene has improved high molecular material compatibility. The method is inexpensive, and has simple and stable operation.