• 专利标题:   Preparing transition metal oxide or graphene composite comprises e.g. mixing transition metal salt, water and solution of graphite oxide dispersed in polyol solvent, and preparing the composite by applying microwaves to the mixed solution.
  • 专利号:   US2012104327-A1, KR2012045411-A
  • 发明人:   KIM K B, KIM H K, KIM J Y
  • 专利权人:   UNIV YONSEI IND ACADEMIC COOP FOUND, UNIV YONSEI IND ACADEMIC COOP FOUND
  • 国际专利分类:   B82B003/00, B82Y099/00, H01B001/18, H01M004/04, H01M004/485, C01B031/02, C01G023/00, H01M010/0525, H01M004/58
  • 专利详细信息:   US2012104327-A1 03 May 2012 H01M-004/485 201231 Pages: 11 English
  • 申请详细信息:   US2012104327-A1 US270132 10 Oct 2011
  • 优先权号:   KR106929

▎ 摘  要

NOVELTY - Preparing a transition metal oxide/graphene composite comprises: (a) mixing a transition metal (M1) salt, water and a solution of graphite oxide dispersed in a polyol solvent; (b) preparing a transition metal (M1) oxide/graphene composite by applying microwaves to the mixed solution; and (c) preparing a transition metal (M1M2) oxide/graphene composite by applying microwaves to a solution obtained by mixing the transition metal (M1) oxide/graphene composite with a transition metal (M2) salt, where M1 and M2 are lithium, ruthenium, nickel, vanadium, cobalt, manganese, iron or titanium. USE - The method is useful for preparing a transition metal oxide/graphene composite, which is used as an anode material for lithium secondary batteries (all claimed). ADVANTAGE - The method provides the transition metal oxide/graphene composite in simplified manner with short manufacturing time, and with high electrochemical performances due to its excellent capacity and rate capability and long lifespan. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for: (1) a lithium titanium oxide/graphene composite having a spinel structure, comprising graphene, and lithium titanium oxide having a nano-sized spinel structure stacked on a surface of the graphene; (2) an anode material for lithium secondary batteries comprising a lithium titanium oxide/graphene composite having a spinel structure; and (3) a lithium secondary battery comprising an electrode formed of an anode material.