• 专利标题:   Producing tungsten trioxide/reduced graphene oxide composite cathode material, comprises e.g. preparing black precursor powder from ammonium metatungstate, reduced graphene oxide and dilute hydrochloric acid to diethylene glycol, and drying.
  • 专利号:   CN108598439-A
  • 发明人:   ZHANG Z, REN Y, LIU J, FAN S, XU J
  • 专利权人:   UNIV KUNMING SCI TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/48, H01M004/583
  • 专利详细信息:   CN108598439-A 28 Sep 2018 H01M-004/36 201871 Pages: 9 Chinese
  • 申请详细信息:   CN108598439-A CN10453430 14 May 2018
  • 优先权号:   CN10453430

▎ 摘  要

NOVELTY - Producing tungsten trioxide/reduced graphene oxide (RGO) composite cathode material, comprises (i) adding ammonium metatungstate, RGO and dilute hydrochloric acid to diethylene glycol to obtain a mixed solution, and then vibrating and dispersing the mixed solution with an ultrasonic generator, (ii) transferring the mixed solution obtained in the step (i) to a reaction vessel for heating, and then naturally cooling to room temperature, and taking out and filtering the mixed solution and washing many times to obtain a black precursor powder, (iii) drying the black precursor powder obtained in the step (2) to obtain a black powder and (iv) placing the black powder obtained in the step (ii) in a microwave oven for calcination, and naturally lowering the temperature to room temperature to obtain black tungsten trioxide/RGO composite powder. USE - The method is useful for producing tungsten trioxide/reduced graphene oxide composite cathode material (claimed). ADVANTAGE - The method produces composite cathode material with small particle size and uniformity, and which exhibits excellent electrochemical performance.