• 专利标题:   Preparing polymer conductive composite hydrogel involves adding pyrrole monomer in graphene oxide aqueous solution, stirring and dispersing by ultrasonic wave to form solution, adding ferrous salt and hydrogen peroxide solution.
  • 专利号:   CN107698914-A
  • 发明人:   HAN Y, LI T, LI W, WANG T, GAO X, ZHANG Z, SONG H, ZHANG C
  • 专利权人:   UNIV SHANDONG SCI TECHNOLOGY
  • 国际专利分类:   C08F220/06, C08F222/38, C08G073/06, C08K003/04, C08L033/02, C08L079/04, H01G011/30, H01G011/36, H01G011/48
  • 专利详细信息:   CN107698914-A 16 Feb 2018 C08L-033/02 201822 Pages: 7 Chinese
  • 申请详细信息:   CN107698914-A CN11089697 08 Nov 2017
  • 优先权号:   CN11089697

▎ 摘  要

NOVELTY - Preparing polymer conductive composite hydrogel involves adding pyrrole monomer in graphene oxide aqueous solution, stirring and dispersing by ultrasonic wave to form solution, adding ferrous salt and hydrogen peroxide solution in obtained solution, stirring and dispersing by ultrasonic wave to form reaction system, placing obtained reaction system at 0-20 degrees C, and stirring for 2 hours, to obtain reactant, adding initiator and N,N'-methylene bisacrylamide, agitating and ultrasonically dispersing uniformly, adding acrylic acid, and continuously stirring for 5-10 minutes. USE - Method for preparing polymer conductive composite hydrogel. DETAILED DESCRIPTION - Preparing polymer conductive composite hydrogel involves adding pyrrole monomer in graphene oxide aqueous solution, stirring and dispersing by ultrasonic wave to form solution, adding ferrous salt and hydrogen peroxide solution in obtained solution, stirring and dispersing by ultrasonic wave to form reaction system, placing obtained reaction system at 0-20 degrees C, and stirring for 2 hours, to obtain reactant, adding initiator and N,N'-methylene bisacrylamide, agitating and ultrasonically dispersing uniformly, adding acrylic acid, and continuously stirring for 5-10 minutes. The reaction is allowed to stand in oven at 70 degrees C, and resulting hydrogel is placed in 45 wt.% hydrogen iodide for reduction, and resulting product is purified and equilibrated in distilled water to obtain final product.