• 专利标题:   Preparing hierarchical structure of zinc oxide-graphene nano-composite involves utilizing graphite, dimethyl formamide and zinc acetate dihydrate as raw materials, and uniformly mixing graphite and concentrated sulfuric acid.
  • 专利号:   CN105692680-A, CN105692680-B
  • 发明人:   LI H, ZHU L
  • 专利权人:   UNIV WUHAN TECHNOLOGY
  • 国际专利分类:   B82Y030/00, C01B031/04, C01G009/02, C01B032/184
  • 专利详细信息:   CN105692680-A 22 Jun 2016 C01G-009/02 201660 Pages: 16 Chinese
  • 申请详细信息:   CN105692680-A CN10105798 26 Feb 2016
  • 优先权号:   CN10105798

▎ 摘  要

NOVELTY - Preparing hierarchical structure of zinc oxide-graphene nano-composite involves utilizing graphite, dimethyl formamide and zinc acetate dihydrate as raw materials. The 1-2g graphite and 20-40mL concentrated sulfuric acid are uniformly mixed and dissolved in 100-200mg sodium nitrate in water bath. The 1.5-3g potassium manganate(VII) is added to ice bath. The 30 wt.% hydrogen peroxide is added to terminate the reaction. The product is washed and dried to obtain flaky graphene oxide. The 43-100mg flaky graphene oxide is dissolved in 150-200ml dimethyl formamide. USE - Method for preparing hierarchical structure of zinc oxide-graphene nano-composite (claimed). ADVANTAGE - The method enables to prepare hierarchical structure of zinc oxide-graphene nano-composite in simple manner that has high light absorbing property. DETAILED DESCRIPTION - Preparing hierarchical structure of zinc oxide-graphene nano-composite involves utilizing graphite, dimethyl formamide and zinc acetate dihydrate as raw materials. The 1-2g graphite and 20-40mL concentrated sulfuric acid are uniformly mixed and dissolved in 100-200mg sodium nitrate in water bath. The 1.5-3g potassium manganate(VII) is added to ice bath. The 30 wt.% hydrogen peroxide is added to terminate the reaction. The product is washed and dried to obtain flaky graphene oxide. The 43-100mg flaky graphene oxide is dissolved in 150-200ml dimethyl formamide. The 0.65-1.5g zinc acetate dihydrate is dissolved in mixture at 85-95 degrees C for 4-6 hours. The obtained product is washed with ethanol and dried to obtain hierarchical structure of zinc oxide-graphene nano-composite.