• 专利标题:   Transition metal oxide nano-particles-containing nano-sheets are made of transition metal phthalocyanine as metal source, graphene oxide as template, hydrazine hydrate as reducing agent and distilled water as medium through calcination.
  • 专利号:   CN106865625-A
  • 发明人:   CHEN Z, WU H, ZHANG J, WU F, XIAO F, WANG B, HE C, WU Y
  • 专利权人:   UNIV HEILONGJIANG
  • 国际专利分类:   B82Y040/00, C01G051/04, C01G053/04, C25B001/04, C25B011/06
  • 专利详细信息:   CN106865625-A 20 Jun 2017 C01G-051/04 201760 Pages: 12 Chinese
  • 申请详细信息:   CN106865625-A CN10079761 14 Feb 2017
  • 优先权号:   CN10079761

▎ 摘  要

NOVELTY - The transition metal oxide nano-particles-containing nano-sheets are made of transition metal phthalocyanine as a metal source, graphene oxide as a template, hydrazine hydrate as a reducing agent and distilled water as a medium, and obtained by calcination. USE - Transition metal oxide nano-particles-containing nano-sheets (claimed). ADVANTAGE - The nano-sheets have unique two-dimensional pleated nano-sheet structure, uniform and smaller size particle layout, and has excellent catalytic performance and excellent stability. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for method for preparing transition metal oxide nano-particles-containing nano-sheets, which involves (i) adding graphene oxide to distilled water, ultrasonically vibrating for 30-50 minutes, adding transition metal phthalocyanine, continuing ultrasonic vibration for 1-4 hours, (ii) then adding hydrazine hydrate, stirring at 10-50? for 1-2 hours, drying the resulting product by centrifugation at 80 degrees C, (iii) and then calcining at 300-600? in air or oxygen atmosphere under the conditions of constant temperature for 1-3 hours, naturally cooling to room temperature, and obtaining nano-sheets composed of transition metal oxide nano-particles.